Effect of Dilute Acid on Hydraulic Fracturing of Carbonate-Rich Shales: Experimental Study

Teklu, Tadesse Weldu (Colorado School of Mines) | Park, Daejin (Korea Gas Corporation and Colorado School of Mines) | Jung, Hoiseok (Korea Gas Corporation and Colorado School of Mines) | Amini, Kaveh (Colorado School of Mines) | Abass, Hazim (Halliburton and Colorado School of Mines)


Tadesse Weldu Teklu, Colorado School of Mines; Daejin Park and Hoiseok Jung, Korea Gas Corporation, and Colorado School of Mines; Kaveh Amini, Colorado School of Mines; and Hazim Abass, Halliburton and Colorado School of Mines Summary Matrix and fracture permeability of carbonate-rich tight cores from Horn River Basin, Muskwa, Otter Park, and Evie Shale formations, were measured before and after exposing the core samples to spontaneous imbibition using dilute acid [1-or 3-wt% hydrochloric acid (HCl) diluted in 10-wt% potassium chloride (KCl) brine]. Permeability and porosity were measured at net stress between 1,000 and 5,000 psia. Brine and dilute-acid imbibition effect on proppant embedment, rock softening/weakening, and fracture roughness were assessed. The following are some of the experiment observations: (a) Formation damage caused by water blockage of water-wet shales can be improved by adding dilute HCl or by using hydrocarbon-based fracturing fluids; (b) matrix permeability of clay-rich or calcite-poor shale samples is usually impaired/damaged by dilute-acid imbibition; (c) matrix permeability and porosity of calcite-rich shales usually improved with dilute-acid imbibition; (d) effective fracture permeability of unpropped calcite-rich shales is reduced by dilute-acid imbibition; the latter is because of "rock softening" and "etching/smoothing" of fracture roughness on the "fracture faces." Nevertheless, dilute-acid imbibition is less damaging than brine (slickwater) imbibition; and (e) proppant embedment was observed during both brine (slickwater) and diluteacid imbibition. Introduction A statistical report in EIA (2016) shows that, in the United States, oil and gas production from tight formations have become increasingly significant since 2007. This is mainly because of the advancement of multistage hydraulic-fracture stimulation in horizontal wells. Even with multistage hydraulic-fracture stimulation horizontal-well technology, oil recovery from tight formations such as the Bakken is usually less than 10% (Alharthy et al. 2015; Sheng 2015; Teklu et al. 2017a). Hence, many researchers are devoted to improving this low oil recovery. Enhanced-oil-recovery studies in tight formations through surfactant and gas injection and acid treatment are among the recent research directions toward improving the ultimate recovery of tight formations or shales (Teklu et al. 2017a, 2018).

  Country: North America > United States (1.00)
  Geologic Time: Phanerozoic > Paleozoic > Devonian (0.68)
  Industry: Energy > Oil & Gas > Upstream (1.00)
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