Whole level of the erosion and the resistance of rocks which were composed closured have been studied, besides, the impact of temperature and laser irradiation for more investigation about this issue has been involved before all. This subject more reveals the matter which laser absorption on the laboratory scale using laser to what extent can cause the augment of the relative permeability and secondary porosity of reservoir rock, that of the vertical and horizontal useful connectivity and eventually that of the positive transferability.
This research has been carried out in the form of case study on one of Iranian south west formations in north east of Behbahan city in Iran, either the rate or generation of forming the subtle and large fractures has been studied by considering and preparing this section from rocks of stratified sequence of the laboratory area before and after the laser irradiation operation and various analyzer by the means of Spectrophotometer and advanced electron microscope. It should be noted that during the erosion and ablation in the laser drilling operation in the experimental rocks of considered field, given the capability of the field, the formation and field lithology we observed the creation of fractures at the level of micro and nano simultaneously whose vacant spaces were positive, and reservoir and some others were neutral, this fractures can be created by the rate of crude oil absorption. The main purpose of this study is to advance the operations towards the higher technology in order to the better efficiency in the field of the well completion to be gained improving the rate of oil production by the introduction of this modern method of improving and fracturing reservoir which uses certain specialized parameters and indicators, and, finally, the certain method that might be a better way to use laser irradiation on our chosen formation of Iran.
Alaskar, Mohammed N. (Stanford University) | Ames, Morgan F. (Stanford University) | Connor, Steve T. (Stanford University) | Liu, Chong (Stanford University) | Cui, Yi (Stanford University) | Li, Kewen (Stanford University) | Horne, Roland N. (Stanford University)
The goal of this research was to develop methods for acquiring reservoir pressure and temperature data near the wellbore and farther out into the formation and to correlate such information to fracture connectivity and geometry. Existing reservoir-characterization tools allow pressure and temperature to be measured only at the wellbore. The development of temperature- and pressure-sensitive nanosensors will enable in-situ measurements within the reservoir. This paper provides the details of the experimental work performed in the process of developing temperature nanosensors. The study investigated the parameters involved in the mobility of nanoparticles through porous and fractured media. These parameters include particle size or size distribution, shape, and surface charge or affinity to rock materials.
The principal findings of this study were that spherically shaped nanoparticles of a certain size and surface charge compatible with that expected in formation rock are most likely to be transported successfully, without being trapped because of physical straining, chemical, or electrostatic effects. We found that tin-bismuth (Sn-Bi) nanoparticles of 200 nm and smaller were transported through Berea sandstone. Larger particles were trapped at the inlet of the core, indicating that there was an optimum particle size range. We also found that the entrapment of silver (Ag) nanowires was primarily because of their shape. This conclusion was supported by the recovery of the spherical Ag nanoparticles with the same surface characteristics through the same porous media used during the Ag nanowires injection. The entrapment of hematite nanorice was attributed to its affinity to the porous matrix caused by surface charge. The hematite coated with surfactant (which modified its surface charge to one compatible with flow media) flowed through the glass beads, emphasizing the importance of particle surface charge.
Preliminary investigation of the flow mechanism of nanoparticles through a naturally fractured greywacke core was conducted by injecting fluorescent silica microspheres. We found that silica microspheres of different sizes (smaller than the fracture opening) could be transported through the fracture. We demonstrated the possibility of using microspheres to estimate fracture aperture by injecting a polydisperse microsphere sample. It was observed that only spheres of 20 µm and smaller were transported. This result agreed reasonably well with the measurement of hydraulic fracture aperture (27 µm), as determined by the cubic law.
On the basis of micro- and mesoscale investigations, a new mathematical formulation is introduced in detail to investigate multiscale gas-transport phenomena in organic-rich-shale core samples. The formulation includes dual-porosity continua, where shale permeability is associated with inorganic matrix with relatively large irregularly shaped pores and fractures, whereas molecular phenomena (diffusive transport and nonlinear sorption) are associated with the kerogen pores. Kerogen is considered a nanoporous organic material finely dispersed within the inorganic matrix. The formulation is used to model and history match gas-permeation measurements in the laboratory using shale core plugs under confining stress. The results indicate significance of molecular transport and strong transient effects caused by gas/solid interactions within the kerogen. In the second part of the paper, we present a novel multiscale perturbation approach to quantify the overall impact of local porosity fluctuations associated with a spatially nonuniform kerogen distribution on the adsorption and transport in shale gas reservoirs. Adopting weak-noise and mean-field approximation, the approach applies a stochastic upscaling technique to the mathematical formulation developed in the first part for the laboratory. It allows us to investigate local kerogenheterogeneity effects in spectral (Fourier-Laplace) domain and to obtain an upscaled "macroscopic" model, which consists of the local heterogeneity effects in the real time-space domain. The new upscaled formulation is compared numerically with the previous homogeneous case using finite-difference approximations to initial/boundary value problems simulating the matrix gas release. We show that macrotransport and macrokinetics effects of kerogen heterogeneity are nontrivial and affect cumulative gas recovery. The work is important and timely for development of new-generation shale-gas reservoir-flow simulators, and it can be used in the laboratory for organic-rich gas-shale characterization.
Clarkson, Christopher R. (University of Calgary) | Wood, James (Encana Corporation) | Burgis, Sinclair (Encana Corporation) | Aquino, Samuel (University of Calgary) | Freeman, Melissa (University of Calgary)
The pore structure of unconventional gas reservoirs, despite having a significant impact on hydrocarbon storage and transport, has historically been difficult to characterize because of a wide poresize distribution (PSD), with a significant pore volume (PV) in the nanopore range. A variety of methods is typically required to characterize the full pore spectrum, with each individual technique limited to a certain pore size range. In this work, we investigate the use of nondestructive, low-pressure adsorption methods, in particular low-pressure N2 adsorption analysis, to infer pore shape and to determine PSDs of a tight gas siltstone reservoir in western Canada. Unlike previous studies, core-plug samples, not crushed samples, are used for isotherm analysis, allowing an undisturbed pore structure (i.e., uncrushed) to be analyzed. Furthermore, the core plugs used for isotherm analysis are subsamples (end pieces) of cores for which mercury-injection capillary pressure (MICP) and permeability measurements were previously performed, allowing a more direct comparison with these techniques. PSDs, determined from two isotherm interpretation methods [Barrett-Joyner-Halenda (BJH) theory and density functional theory (DFT)], are in reasonable agreement with MICP data for the portion of the PSD sampled by both. The pore geometry is interpreted as slot-shaped, as inferred from isotherm hysteresis loop shape, the agreement between adsorption- and MICP-derived dominant pore sizes, scanning-electron-microscope (SEM) imaging, and the character of measured permeability stress dependence. Although correlations between inorganic composition and total organic carbon (TOC) and between dominant pore-throat size and permeability are weak, the sample with the lowest illite clay and TOC content has the largest dominant pore-throat size and highest permeability, as estimated from MICP. The presence of stress relief-induced microfractures, however, appears to affect laboratory-derived (pressure-decay and pulse-decay) estimates of permeability for some samples, even after application of confining pressure. On the basis of the premise of slot-shaped pore geometry, fractured rock models (matchstick and cube) were used to predict absolute permeability, by use of dominant pore-throat size from MICP/adsorption analysis and porosity measured under confining pressure. The predictions are reasonable, although permeability is mostly overpredicted for samples that are unaffected by stressrelease fractures. The conceptual model used to justify the application of these models is slot pores at grain boundaries or between organic matter and framework grains.
Acharya, Mihir Narayan (Kuwait Oil Company) | Kabir, Mir Md Rezaul (Kuwait Oil Company) | Al-Ajmi, Saad Abdulrahman Hassan (Kuwait Oil Company) | Pradhan, San Prasad (Kuwait Oil Company) | Dashti, Qasem M. (Kuwait Oil Company) | Al-anzi, Ealian H.D. (Kuwait Oil Company) | Chakravorty, Sandeep (Schlumberger)
The deep, sub-salt reservoir complex is tiered with fractured tight carbonate at bottom and top, with the two sub-units of "upper unconventional kerogen?? and "lower inter-bedded kerogen-carbonate?? in the middle. This depositional setting is challenging for horizontal well placement where the thicknesses of respective sub-units are about 50 and 30 feet with varying geomechanical and petrophysical properties. Additionally, this complexity poses limitations in completions and effective stimulation of the Kimmeridgian-Oxfordian reservoirs in several gas fields at development stage in Kuwait.
A horizontal well is placed in the lower sub-unit of the laminated complex of unconventional kerogen and fractured carbonate reservoir as a Maximum Reservoir Contact (MRC) type well. A pilot mother-bore was drilled and logged to identify the lithological properties across the entire vertical domain - facilitates the optimization of horizontal drain-hole placement within the targeted reservoir units.
No wellbore stability issues in drilling were predicted based on the geomechanical understanding where core-calibrated logs from offset vertical wells were considered. However, this modeling method did not have the functionality to integrate the impact of drawdown on the laminated formation which became unstable and collapsed during the short open-hole drill-stem test (DST) plugging the tubing prior to the final completions. An alternative "book-shelf?? geomechanical model was considered at pre-drill stage for predicting the wellbore stability. Once the drilling was completed, the time-lapsed multi-arm caliper indicated the validity of the alternative methodology in predicting the unstable stack of laminations in kerogen-rich strata.
The paper discusses an optimization methodology to enhance the understanding of static and dynamic geomechanical stability through the use of BHI data. Objective of the proposed method is to help improve the effectiveness of completions where wellbore stability due to geomechanical complexity in stacked-pay reservoirs is a primary wellbore challenge in deploying the completions and executing a subsequent stimulation and testing campaign.
Waterflooding has been the most popular post-primary production approach for improving oil recovery. In fractured reservoirs with large structural relief, gas injection can produce much of the post-waterflood remaining oil by gravity drainage. Oil recovery by gas-invoked gravity drainage in waterflooded reservoirs is known as the double displacement process (DDP). One major reason, among many, is that the three-phase relative permeability residual oil saturation endpoint is generally smaller than the residual oil saturation endpoint for the water-oil displacement.
Field data indicate that the DDP has been successful in single-porosity sandstone formations. Intuitively, one can expect that DDP should produce similar results in reservoirs with ample intercommoned vertical fractures, which is the objective of this work. With the aid of tests on tight reservoir cores from a major Middle East carbonate reservoir, this study focuses on evaluating the DDP in fractured carbonate reservoirs where the wettability ranges from neutral to oil-wet conditions. The scope of the study includes: (1) assessment of the DDP experimentally in fractured cores using a high-speed centrifuge, (2) simulating the experiments numerically, and (3) upscaling laboratory results to field applications.
Results from water-oil gravity drainage tests followed by gas-oil gravity drainage in fractured and unfractured cores are presented. We also show numerical simulation results of matching the experiments using both transfer function and 2-D numerical simulation, and how results from our study can be used in field applications.
Typical waterflood oil recovery from 0.1-md to 2-md fractured carbonate cores has been noted to be around 38% of the initial oil in place while incremental additional oil recovery for gas-oil gravity drainage is nearly as much as the recovery from water.
Our studies of the underlying fundamental gas-recovery mechanisms from shale gas are motivated by expectations of the increasing role of shale gas in national energy portfolios worldwide. We use pore-scale analysis of reservoir shale samples to identify critical parameters to be employed in a gas-flow model used to evaluate well-production data. We exploit a number of 3D-imaging technologies to study the complexity of shale pore structure: from low-resolution X-ray computed tomography (CT) to focused ion beam and scanning electron microscopy (FIB/SEM). We observe that heterogeneity is present at all scales. The CT data show fractures, thin layers, and density heterogeneity. The nanometer-scale-resolution FIB/SEM images show that various mineral inclusions, clays, and organic matter are dispersed within a volume of few-hundred µm3. Samples from different regions differ sharply in the shape, size, and distribution of pores, solid grains, and the presence of organic matter. Although the samples have clearly distinguishable signatures related to the regions of origin, extremely low permeability is a common feature. This and other pore-scale observations suggest a bounded-stimulated-domain model of a horizontal well within fractured shale that accounts for both compression and adsorption gas storage. Using the method of integral relations, we obtain an analytical formula approximating the solution to the pseudopressure diffusion equation. This formula makes fast and simple evaluation of well production possible without resorting to complex computations. It ss a decline curve, which predicts two stages of production. During the early stage, the production rate declines with the reciprocal of the square root of time, whereas later, the rate declines exponentially. The model has been verified by successfully matching monthly production data from a number of shale-gas wells collected over several years of operation. With appropriate scaling, the data from multiple wells collapse on a single type curve. Pore-scale image analysis and the mesoscale model suggest a dimensionless adsorption-storage factor (ASF) to characterize the relative contributions of compression and adsorption gas storage.
This article, written by Editorial Manager Adam Wilson, contains highlights of paper SPE 157031, "Application of Nanotechnology in Drilling Fluids," by Katherine Price Hoelscher, SPE, Guido De Stefano, SPE, Meghan Riley, SPE, and Steve Young, SPE, M-I SWACO, prepared for the 2012 SPE International Oilfield Nanotechnology Conference and Exhibition, Noordwijk, The Netherlands, 12-14 June. The paper has not been peer reviewed.
Fracture fluid flow back has been identified as one of the major challenges of hydraulic fracturing operations conducted in shale reservoirs. Factors causing the very low fracture fluid recovery need to be well understood and properly addressed, in
order to get full benefits from costly hydraulic fracture jobs conducted in unconventional reservoirs. Despite the recent surge of investigations of the problem, one major question still remains: what happens to the fracture fluid that is not recovered?
Does it stay in the fracture or does it go into the matrix? In case of both mechanisms are responsible for fracture fluid retainment, what fraction of fracture fluid stays in the propped fracture and what fraction is transferred from fracture to
matrix. The focus of the current study is to understand if the transfer of fracture fluid from fracture to matrix through imbibition is of significant importance.
We systematically measure the imbibition rate of water, brine, and oil into the actual core samples from the three shale sections of Horn River basin (i.e., Fort Simpson, Muskwa and Otter Park). We characterize the shale samples by measuring,
porosity, wettability, mineral composition through XRD analysis, and interpreting the well log data. The results show that imbibition could be a viable mechanism for fluid transfer from fracture to matrix in Horn River shales. The comparative study shows the imbibition rate in the direction parallel to the bedding plane is higher than that in the direction perpendicular to the bedding. The study also suggests that the imbibition rate of the aqueous phases is significantly
higher than that of the oleic phases.