Abstract This study falls in the context of underground coal fires (UCF) where burning coal can elevate the temperature of a rock mass in excess of thousand degrees. The objective of the research was to experimentally investigate the change in mechanical behavior of a rock when subjected to temperatures up to 900 °C. Several blocks of an Australian mudstone were collected from a mining site in New South Wales, Australia. X-ray diffraction and thermal-gravimetric analysis were conducted on powdered rock in order to determine the critical temperatures at which the main mineralogical changes occur. Then, cylindrical specimens were prepared from intact rock blocks for unconfined compression tests. These rock specimens were then treated by heating in a temperature-controlled furnace at temperatures varying from 100 °C to 900 °C. The heating process consisted of two stages: raising temperature with very slow rate of 1 °C per hour followed by a holding period of 24 hours and then a slow cooling process to room temperature. The compression tests were carried out on treated rock specimens to characterize the change in compressive strength. The macroscopical study was complemented by microstructural investigations via optical microscope, scanning electron microscope (SEM) and mercury intrusion porosimetry (MIP). Results show that the unconfined compressive strength of mudstone decreases with increasing heating temperature up to 450 °C, beyond which it increases. This can be explained by the combined effects of micro cracks and mineral thermal reactions caused by heating process.
Introduction Underground coal fires (UCFs) are a serious environmental problem of global dimension. These fires, which can result from human activity (in most cases through mining activities) or occur naturally, are problematic for many reasons including loss of valuable non-renewable resources, mine safety, damage to infrastructure and damage to the natural environment (Stracher & Taylor, 2004; Sinha & Singh, 2005; Kuenzer et al., 2007). This is why underground coal fires have been of great concern to scientists and engineers (Voigt & Rüter, 2005). UCFs are characterized by very slow burning kinetics due to the limited availability of oxygen underground and very elevated temperature at the core of the fire because of surrounding ground preventing heat dissipation. Temperatures at combustion center of UCFs of up to 1300 °C have been reported in the literature (Stracher & Taylor, 2004). The continuous combustion of the coal seam typically leads to a progressive collapse of the overburden soil/rock mass, that is left unsupported, and to the formation of large cracks, which provide new air circulation paths allowing the fire to propagate (Ide et al., 2010).